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Influence of growth ambience and doping on the structural properties of multiferroic DyMnO3

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1 January 2013
Publication year: 2013
Source:Journal of Crystal Growth, Volume 362

We report on the single crystal growth of 50% Sr and Y doped multiferroic DyMnO3 using optical floating zone technique. A comparison of the effect of growth ambience and of chemical substitution on the crystal structure of DyMnO3 is attempted. It is observed that DyMnO3 adopts Pm3m cubic structure with 50% Sr doping whereas with 50% Y doping, the crystal structure is hexagonal P 6 3 cm . Orthorhombic Pnma structure is adopted by DyMnO3 when grown in air, whereas hexagonal P 6 3 cm structure is obtained when grown under the ambience of argon. The structural polymorphism is discussed in terms of difference in ionic sizes of Sr, Y and Dy, comparable Gibbs free energies and coordination schemes of surrounding oxygens for hexagonal and orthorhombic structures of DyMnO3.

Highlights

► We study the effect of doping divalent, non-magnetic Sr and Y in multiferroic DyMnO3. ► Crystal structure changes to cubic Pm3m with Sr doping. ► Hexagonal P 6 3 cm structure results with Y doping. ► Sr doped system is a spin glass. ► Y doped compound is a frustrated antiferromagnet.

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